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Application of NQS in Pharmaceutical Analysis   Abdalla Elbashir

Application of NQS in Pharmaceutical Analysis

116 страниц. 2012 год.
LAP Lambert Academic Publishing
This book demonstrates the potential of 1,2-Naphthoquinone-4-sulphonic acid sodium salt (NQS) as an analytical reagent for the analysis of pharmaceutical drugs bearing amine group in their pharmaceutical formulation. Simple, fast and reliable spectrophotometric methods were developed and validated for the determination of various pharmaceuticals bearing amine group ,cephalosporin, fluoroquinolones, cardiovascular drugs and antimalarial. Different variables affecting the reactions between the NQS and the drug bearing amine group such as pH, concentration of NQS, temperature, and reaction time were carefully studied and optimized. The methods developed were validated with respect to accuracy, precision, linearity, selectivity, sensitivity, limit of detection, and limit of quantification according to the International Conference of Harmonization (ICH) guidelines for validation of analytical procedures. The proposed methods were successfully applied to the determination of each...
 
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